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101.
本文研究了新席夫碱吡哆醛缩邻氨基酚的合成及其分析应用,提出了钒(V)的分光光度测定法,该法简便,灵敏,选择性好。 相似文献
102.
脉冲染料激光器的可见光波段辐射通过共线倍频和非共线混频实现紫外波段的连续可调谐输出.本文报道了一种闭环跟踪方法;在调谐起始波长处,将取样光束在垂直相位匹配方向分割成等光强的两部分,然后在波长调谐时比较和平衡这两部分光强.对该方法在理论上作了分析并在实验中得到成功的验证.获得的自动跟踪效率大于90%. 相似文献
103.
我们对多电子束契伦柯夫自由电子激光进行了首次实验研究。280A,500kV的电子束被引入一多介质矩形谐振腔,在频率为33.4GHz处产生了1.7MW的契伦柯夫相干受激辐射。互作用效率为1.2%。 相似文献
104.
研究了乘积空间中严格集压缩减算子不动点存在唯一性问题,在弱连续的条件下,得到了不动点的存在唯一性和迭代收敛性.并给出了它的应用. 相似文献
105.
Andreas Wallner Margit Hölbling Judith Baumgartner Christoph Marschner 《Silicon Chemistry》2007,3(3-4):175-185
A number of cyclo-and bicyclosilanes have been prepared and structurally characterized by X-ray crystallography and Raman
spectroscopy. 1,1,4,4- and 1,1,3,3-tetrakis(trimethylsilyl)octamethylcyclohexasilanes were found to exhibit unusual twist- and twisted boat-conformations. The UV absorption properties of all compounds were studied and found to show absorption maxima red shifted
compared to the parent compound dodecamethylcyclohexasilane.
Dedicated to Prof. Mitsuo Kira on the occasion of his reception of the Wacker Silicon Award 2005 and in recongnition of his
numerous outstanding achievements in organosilicon chemistry. 相似文献
106.
用共沉淀法制备了Mg2 + 掺杂的In2 O3 纳米粉 ,研究了镁掺杂对In2 O3 电导和气敏性能的影响 .结果表明 :MgO和In2 O3 间可形成有限固溶体In2 -xMgxO3 (0≤x≤ 0 .40 ) ;MgIn× 电离的空穴对材料导带电子的湮灭 ,使掺镁纳米粉的电导变得很小 ;n(Mg2 + )∶n(In3 + ) =1∶2共沉淀物于 90 0℃下热处理 4h ,用所得的纳米粉制作的传感器在 32 0~ 370℃下 ,对 45 μmol/LC2 H5OH的灵敏度达 10 2 .5 ,为相同浓度干扰气体Petrol的 12倍多 . 相似文献
107.
A. Hansen M.H. Jensen K. Sneppen G. Zocchi 《The European Physical Journal B - Condensed Matter and Complex Systems》1998,6(1):157-161
We present a statistical mechanics treatment of the stability of globular proteins which takes explicitly into account the
coupling between the protein and water degrees of freedom. This allows us to describe both the cold and the warm unfolding,
thus qualitatively reproducing the known thermodynamics of proteins.
Received: 19 March 1998 / Revised and Accepted: 25 May 1998 相似文献
108.
M. Stenger S. Baumhoff J.-Y. Prieur J. Joffrin J.-P. Contour 《The European Physical Journal B - Condensed Matter and Complex Systems》1998,2(2):177-182
We present measurements of the attenuation and phase velocity of surface acoustic waves in thin YBa2Cu3O films as a function of temperature, in magnetic fields up to 3.6 T applied parallel to the c-axis of the films. We have observed anomalies in both, the attenuation and the phase velocity in the vicinity of the superconducting
critical temperature which do not depend on the magnetic field. Possible origins of these anomalies, observed, to our knowledge,
for the first time in YBa2Cu3O thin films, are discussed and compared to bulk acoustic wave experiments. We present a kind of feedback technique for surface
acoustic waves which improves the sensitivity of this type of measurement. The actual sensitivity limits are mentioned.
Received: 7 August 1997 / Revised: 7 November 1997 / Accepted: 17 November 1997 相似文献
109.
C. Ruyer-Quil P. Manneville 《The European Physical Journal B - Condensed Matter and Complex Systems》1998,6(2):277-292
A new model of film flow down an inclined plane is derived by a method combining results of the classical long wavelength
expansion to a weighted-residuals technique. It can be expressed as a set of three coupled evolution equations for three slowly
varying fields, the thickness h, the flow-rate q, and a new variable that measures the departure of the wall shear from the shear predicted by a parabolic velocity profile. Results of a preliminary
study are in good agreement with theoretical asymptotic properties close to the instability threshold, laboratory experiments
beyond threshold and numerical simulations of the full Navier-Stokes equations.
Received: 16 April 1998 / Revised: 29 June 1998 / Accepted: 2 July 1998 相似文献
110.
A. Barnabé A. Maignan M. Hervieu B. Raveau 《The European Physical Journal B - Condensed Matter and Complex Systems》1998,1(2):145-150
Doping of Mn-site by chromium, cobalt and nickel has been investigated in the calcium rich manganites and
. Whatever the nature of the doping element, a rapid disappearance of the charge ordered (CO) state is observed, decreasing as the doping rate increases. But the most important result concerns the Cr-doped compounds for which a re-entrant insulator to metal transition at 90-120 K is observed for x
=0.10-0.12, in a zero magnetic field. The possibility to induce colossal magnetoresistance (CMR) properties for high (IV) contents ((IV)/) for x
=0.07-0.12 is shown for the first time, the resistance ratios reaching at 30 K. This study also shows differently that the small size of the A-site cation (Pr, Ca) is not a redhibitory obstacle
to the appearance of CMR properties in manganites, in contrast with previously established phase diagrams.
Received: 18 June 1997 / Revised: 4 August 1997 / Accepted: 10 November 1997 相似文献